By Zhong Lin Wang
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Extra info for Handbook of Nanophase and Nanostructured Materials Vol. 2 : Characterization
Example text
The area contributing to diffraction is controlled by the probe size. 2 nm, nanodiffraction can therefore be readily achieved from an area smaller than the size of the unit cell. When the probe is focused, minimum probe size can be obtained. The diffraction spots in the diffraction pattern are disks instead of sharp spots. The diameter of the disk is defined by the semiconvergent angle of the electron beam. This could cause overlapping of spots if the unit cell is large. The sharp spots pattern can be obtained by defocusing the probe slightly using the condenser lens as shown in Fig.
The thermodynamic properties of Au nanorods are an example. , 1997). A series of in situ TEM images recorded for the same specimen region as the temperature was increased continuously from room temperature to 923 K, showing the formation process of Au small nanoparticles on the carbon support in Fig. 28(a—h). Nucleation started at 473 K as shown in Fig. 28(b) and it was only observed by TEM at 488 K, shown in Fig. 28(c). It is clear that as the temperature reached 433 K, at which the structure of the micelles around the rods was found to collapse in solution, no visible change was observed in the morphology of the nanorods.
There are some atom-high surface steps on the {111} surfaces and the corners. These atomic-scale structures are likely important for enhancing the catalysis activities of the nanocrystals. 8 HRTEM images of truncated tetrahedral Pt nanocrystals oriented along 110 . 2 Twinning Structure and Stacking Faults Twinning is one of the most popular planar defects in nanocrystals, and it is frequently observed for fcc structured metallic nanocrystals. Twinning is the result of two subgrains sharing a common crystallographic plane, thus, the structure of one subgrain is the mirror reflection of the other by the twin plane.